Ghernaouti F. auteur aut IRD Perrin Aurélie auteur aut IRD Causse J. auteur aut IRD Chandre Fabrice auteur aut IRD Cornu D. auteur aut IRD Cambedouzou J. auteur aut IRD text journalArticle eng text/pdf born digital access Encapsulation of active substances in biopolymer beads becomes a widely developed approach to gain efficiency for many applications. However, the characterization of such aqueous materials in their early stage of production is very delicate regarding their textural properties. The classical tools such as gas adsorption and Hg porosimetry can hardly provide relevant information since they require the removal of water, which is yet a fundamental part of the sample that drives its structure. In this article, we used small angle x-ray scattering (SAXS) as a tool in order to determine the specific surface area (SSA) of alginate microbeads in solution. This has been made possible by a careful procedure of SAXS measurements, involving calibration samples, allowing writing intensities in absolute units. Therefore, the Porod limit theory was used to calculate the SSA from the scattering length contrast and the measured absolute intensity. In addition, we compared the SSA of microbeads obtained from pure water and from a widely used cell culture medium, and we followed the textural evolution of a water alginate sample during the first step of a gentle drying process. Our results show that SAXS should be considered as a valuable tool for physico-chemists and food formulators in order to extract in situ dimensional and textural information of hydrogels during the formulation. It enables them to figure out the real surface available for the sorption of additive or active molecules in the formulation of biopolymers such as alginates, empowering them to better control encapsulation processes. specialized Alginate beads Texture analysis Small angle scattering Specific surface area 020 054 127 107498 [6 ] 2022 0268-005X https://www.documentation.ird.fr/hor/fdi:010083943 10.1016/j.foodhyd.2022.107498 0268-005X [F B010083943] https://www.documentation.ird.fr/hor/fdi:010083943 https://www.documentation.ird.fr/intranet/publi/2022-02/010083943.pdf Accès réservé (Intranet de l'IRD) IRD - Base Horizon / Pleins textes 2022-02-04 2025-02-24 fdi:010083943 fre